Practical Approach for Clean Preparation of Z-β-Thiocyanate Alkenyl Esters

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成果类型：

期刊论文

作者：

Wu, Chao;Hong, Lin;Shu, Hui;Zhou, Qun-Huai;Wang, Yi;...

通讯作者：

He, Wei-Min

作者机构：

[Wang, Yi; Wu, Chao; Hong, Lin; Shu, Hui; He, Wei-Min; Zhou, Qun-Huai] Hunan Univ Sci & Engn, Dept Chem, Yangzi Tan Rd 130, Yongzhou 425100, Peoples R China.

[Su, Neng] Hunan Univ Sci & Technol, Minist Educ, Key Lab Theoret Organ Chem & Funct Mol, Taoyuan Rd 1, Xiangtan 411201, Peoples R China.

[Jiang, Si; Wu, Chao; Cao, Zhong] Changsha Univ Sci & Technol, Hunan Prov Key Lab Mat Protect Elect Power & Tran, Wanjiali Rd 960, Changsha 410114, Hunan, Peoples R China.

通讯机构：

[He, Wei-Min] H

Hunan Univ Sci & Engn, Dept Chem, Yangzi Tan Rd 130, Yongzhou 425100, Peoples R China.

语种：

英文

关键词：

Biomass;Prevention;Propargylic carboxylates;Lactic acid;Liquid separation

期刊：

ACS SUSTAINABLE CHEMISTRY & ENGINEERING

ISSN：

2168-0485

年：

2019

卷：

期：

页码：

8798-8803

DOI：

10.1021/acssuschemeng.9b00708

基金类别：

We are grateful for financial support from the Hunan Provincial Natural Science Foundation of China (Nos. 2019JJ20008 and 2019JJ50194) and the construct program of applied characteristic discipline in Hunan University of Science and Engineering.

机构署名：

本校为其他机构

院系归属：

化学与生物工程学院

摘要：

A practical and eco-friendly method for the clean preparation of a variety of Z-β-thiocyanate alkenyl esters via lactic acid-catalyzed multicomponent hydrothiocyanation reaction was established. In the subgram-scale synthesis, Z-β-thiocyanate alkenyl esters were exclusively generated, and the product could be easily isolated in high purity via extraction. In the large-scale synthesis, the pure products could be simply collected through liquid-liquid separation. The eco-friendly lactic acid played a dual function in the transformation, serving...

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