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Ultrasound-promoted Brønsted acid ionic liquid-catalyzed hydrothiocyanation of activated alkynes under minimal solvent conditions

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成果类型:
期刊论文
作者:
Wu, Chao;Lu, Ling-Hui;Peng, Ai-Zhong;Jia, Guo-Kai;Peng, Cun;...
通讯作者:
He, Wei-Min
作者机构:
[Wu, Chao; He, Wei-Min; Peng, Ai-Zhong; Jia, Guo-Kai; Peng, Cun] Hunan Univ Sci & Engn, Hunan Prov Engn Res Ctr Ginkgo Biloba, Yongzhou 425100, Peoples R China.
[He, Wei-Min; Xu, Xinhua; Lu, Ling-Hui] Hunan Univ, State Key Lab Chemo Biosensing & Chemometr, Changsha 410082, Hunan, Peoples R China.
[Wu, Chao; Cao, Zhong] Changsha Univ Sci & Technol, Hunan Prov Key Lab Mat Protect Elect Power & Tran, Changsha 410114, Hunan, Peoples R China.
[Tang, Zilong] Hunan Univ Sci & Technol, Key Lab Theoret Organ Chem & Funct Mol, Minist Educ, Xiangtan 411201, Peoples R China.
通讯机构:
[He, Wei-Min] H
Hunan Univ Sci & Engn, Hunan Prov Engn Res Ctr Ginkgo Biloba, Yongzhou 425100, Peoples R China.
Hunan Univ, State Key Lab Chemo Biosensing & Chemometr, Changsha 410082, Hunan, Peoples R China.
语种:
英文
期刊:
Green Chemistry
ISSN:
1463-9262
年:
2018
卷:
20
期:
16
页码:
3683-3688
基金类别:
We are grateful for financial support from the post-funded projects of Hunan University of Science and Engineering, the National Natural Science Foundation of China (No. 21372070, 21273068, 21545010 and 21302048), the Scientific Research Hunan Provincial Education Department (No. 15C0464), the Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province (2012-318).
机构署名:
本校为其他机构
院系归属:
化学与生物工程学院
摘要:
By using water as the hydrogen source, an eco-friendly and practical protocol for the synthesis of Z-vinyl thiocyanates through ultrasound-promoted Brønsted acid ionic liquid-catalyzed hydrothiocyanation of activated alkynes under minimal solvent conditions has been developed. This process effectively avoids the use of organic solvents, metal catalysts and harsh reaction conditions. This reaction shows attractive characteristics such as operational simplicity, broad substrate scope with good to excellent yields, ease of scale-up and high energy efficiency and recy...

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