In order to consider the performance enhancement and feasibility of practical application, this research work discussed the effects of different ions on the photocatalytic activity of TiO2/Fe2O3 hybrids in detail, involving H +, OH−, NH 4+, and NO 3−. The TiO2/Fe2O3 hybrids were prepared by organic electrolyte-assisted sol–gel method under UV irradiation, and their function mechanisms were analyzed. Experiment results show that the resultant TiO2/Fe2O3 hybrids possess excellent photocatalytic activity and photocatalytic stability for degrada...