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Shape-controlled growth of In(OH)3 crystals synthesized by diglycol-mediated solvothermal process

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成果类型:
期刊论文
作者:
Chen, S. G.*;Huang, Y. F.;Cheng, Y.;Xia, Q.;Liao, H. W.;...
通讯作者:
Chen, S. G.
作者机构:
[Chen, S. G.; Liao, H. W.; Long, C. G.; Xia, Q.; Cheng, Y.] Changsha Univ Sci & Technol, Sch Mat Sci & Engn, Changsha 410076, Hunan, Peoples R China.
[Huang, Y. F.] Hunan Univ, Sch Mat Sci & Engn, Changsha 410082, Hunan, Peoples R China.
通讯机构:
[Chen, S. G.] C
Changsha Univ Sci & Technol, Sch Mat Sci & Engn, Changsha 410076, Hunan, Peoples R China.
语种:
英文
关键词:
Crystal growth;Crystal structure;Phase structure;Solvation;X ray powder diffraction;Crystal directions;Indium hydroxide;Shape controlled growth;Solvothermal processes;Indium compounds
期刊:
Materials Letters
ISSN:
0167-577X
年:
2008
卷:
62
期:
10-11
页码:
1634-1637
基金类别:
The authors are very much grateful to CSUST (Changsha University of Science and Technology) for financial support under Contract No. 1004086 and for giving permission to publish this work.
机构署名:
本校为第一且通讯机构
院系归属:
材料科学与工程学院
摘要:
In(OH)3 and InOOH crystals were synthesized at different temperatures by diglycol-mediated solvothermal processes. Their phase structures, morphologies and growth mechanisms were investigated by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and chemical analysis. A small quantity of ((H2O)3In)Cl3 was observed in In(OH)3 crystals, which resulted in formation of In(OH)3 crystals with complicated shapes and morphologies. In(OH)3 grew along [1 0 0] direction, while ((H2O)3In)Cl3 grew preferentially along several crystal directi...

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