Synthesis of pyridyl derivatives for the future functionalization of biomolecules labeled with the fac-[Re-188(CO)(3)(H2O)(3)](+) precursor

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成果类型：

期刊论文

作者：

Xia, Jiaoyun*;Wang, Yongxian;Li, Gucai;Yu, Junfeng;Yin, Duanzhi

通讯作者：

Xia, Jiaoyun

作者机构：

[Xia, Jiaoyun] Changsha Univ Sci & Technol, Coll Chem & Environm Engn, Changsha 410076, Hunan, Peoples R China.

[Wang, Yongxian; Yu, Junfeng; Yin, Duanzhi] Chinese Acad Sci, Shanghai Inst Appl Phys, Radiopharmaceut Ctr, Shanghai 201800, Peoples R China.

[Li, Gucai] Hunan Inst Engn, Dept Chem & Chem Engn, Xiangtan 411101, Hunan, Peoples R China.

[Xia, Jiaoyun] Changsha Univ Sci & Technol, Coll Chem & Environm Engn, 45 Chiling Rd, Changsha 410076, Hunan, Peoples R China.

通讯机构：

[Xia, Jiaoyun] C

Changsha Univ Sci & Technol, Coll Chem & Environm Engn, 45 Chiling Rd, Changsha 410076, Hunan, Peoples R China.

语种：

英文

关键词：

Absolute Methanol;Iminodiacetic Acid;Bromoacetic Acid;Tricarbonyl Complex;Tetraethylammonium Bromide

期刊：

Journal of Radioanalytical and Nuclear Chemistry

ISSN：

0236-5731

年：

2009

卷：

279

期：

页码：

245-252

DOI：

10.1007/s10967-007-7145-8

基金类别：

National Natural Science Foundation of China [10405034, 20501022]

机构署名：

本校为第一且通讯机构

院系归属：

化学与生物工程学院

摘要：

In this paper, we investigated three ligand systems, symmetric and asymmetric pyridyl-containing tridentate ligands (L1NH2 = (bis(2-pyridylmethyl)-amino)-ethylamine, L2H = (bis(2-pyridylmethyl)-amino)-acetic acid, L3NH2 = [(6-amino-hexyl)-pyridyl-2-methyl-amino]-acetic acid) as bifunctional chelating agents for labeling biomolecules. These ligands reacted with the precursor fac-[188Re(CO)3(H2O)3]+ and yielded the radioactive complexes fac-[188Re(CO)3L] (L = three ligands), which were identified by RP-HPLC. The corresponding stable rhenium trica...

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Synthesis of pyridyl derivatives for the future functionalization of biomolecules labeled with the fac-[Re-188(CO)(3)(H2O)(3)](+) precursor

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