Heat capacities and thermodynamic properties of (S)-tert-butyl 1-phenylethylcarbamate

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期刊论文

作者：

Zeng, Ju-Lan*;Yu, Sai-Bo;Tong, Bo;Sun, Li-Xian;Tan, Zhi-Cheng;...

通讯作者：

Zeng, Ju-Lan

作者机构：

[Zeng, Ju-Lan; Cao, Zhong; Yang, Dao-Wu] Changsha Univ Sci & Technol, Hunan Prov Key Lab Mat Protect Elect Power & Tran, Changsha 410114, Hunan, Peoples R China.

[Yu, Sai-Bo] China Tobacco Hunan Ind Corp, Changsha 410007, Hunan, Peoples R China.

[Tong, Bo] Dalian Univ Technol, Sch Chem Engn, Dept Chem, Dalian 116023, Peoples R China.

[Sun, Li-Xian; Tan, Zhi-Cheng] Chinese Acad Sci, Dalian Inst Chem Phys, Thermochem Lab, Dalian 116023, Peoples R China.

[Zhang, Jing-Nan] Heilongjiang E Coll, Dept Food & Environm Engn, Haerbin 150086, Peoples R China.

通讯机构：

[Zeng, Ju-Lan] C

Changsha Univ Sci & Technol, Hunan Prov Key Lab Mat Protect Elect Power & Tran, Changsha 410114, Hunan, Peoples R China.

语种：

英文

关键词：

(S)-tert-butyl 1-phenylethylcarbamate;Phase transition;Adiabatic calorimetry;DSC;TG

期刊：

Journal of Thermal Analysis and Calorimetry

ISSN：

1388-6150

年：

2011

卷：

103

期：

页码：

1087-1093

DOI：

10.1007/s10973-010-1155-4

基金类别：

National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21003014, 21075011, 20775010]; Hunan Provincial Science and Technology Project [2010FJ3167]; Hunan Provincial Natural Science Foundation of ChinaNatural Science Foundation of Hunan Province [09JJ3016]; Ministry of Education of the People's Republic of ChinaMinistry of Education, China [NCET-10-0138]; Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation (Changsha University of Science Technology) [2010CL07]; Changsha University of Science Technology

机构署名：

本校为第一且通讯机构

院系归属：

化学与生物工程学院

摘要：

An N-tert-butyloxycarbonylated organic synthesis intermediate, (S)-tert-butyl 1-phenylethylcarbamate, was prepared and investigated by means of differential scanning calorimetry (DSC) and thermogravimetry (TG). The molar heat capacities of (S)-tert-butyl 1-phenylethylcarbamate were precisely determined by means of adiabatic calorimetry over the temperature range of 80-380 K. There was a solid–liquid phase transition exhibited during the heating process with the melting point of 359.53 K. The molar enthalpy and entropy of this transition were d...

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Heat capacities and thermodynamic properties of (S)-tert-butyl 1-phenylethylcarbamate

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