期刊论文

Chen, S. G.

英文

Materials Letters

0167-577X

2008

62

16

2503-2506

10.1016/j.matlet.2007.12.032

The authors are very much grateful to CSUST (Changsha University of Science and Technology) for financial support under Contract No. 1004086 and for giving permission to publish this work.

本校为第一且通讯机构

Cuprous sulfide (Cu2-xS) crystals in different stoichiometries were synthesized by hydro- and solvo-thermal methods at 125°C using Na2S2O3 as sulfur source in pure water, mixed solvents of ethylenediamine (en) and water, and pure en, respectively. The products were characterized by X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersion spectrometer (EDS), transmission electron microscope (TEM) and selected area electronic diffraction (SAED). Owing to different sulfur sources, crystal structures a...